
|
Machine Name |
nmr500 |
Location |
Stauffer I 18A |
Hardware |
500 MHz NMR spectrometer
Varian Inova console
Dell
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Software |
RHEL 6.3
VNMRJ 4.2 |
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Primary Uses of Instrument |
1) 1D 1H, 13C, 19F, 31P, other nuclei
2) 1D NOE
3) 1D with variable temperature (-100º - 150ºC)
4) All 2D experiments including COSY, TOCSY, HSQC, HMBC, ROESY, NOESY
5) Solvent Suppression |
Probes |
5mm PFG Switchable (Standard Probe)
X/H
Tunable to X nuclei from 31P (202 MHz) to 15N (50 MHz)
1H channel tunable to 19F
Ideal for detection of broadband nuclei Can be used for most 2D experiments including COSY, TOCSY, HSQC, HMBC, ROESY, NOESY, but less sensitive than inverse type probes 5mm Triple Resonance/Triax Pulsed Field Gradient
HCN Ideal for Proton detect experiments, especially 2D and 3D experiments Including: NOESY/ROESY/TOCSY (1H/1H) HMQC/HSQC/HMBC (1H/13C or 1H/15N)
3mm Triple Resonance/Z Pulsed Field Gradient HCN Ideal for Proton detect experiments with small sample volumes
5mm Double Resonance/Z Pulsed Gradient H/X Ideal for Proton detect experiments especially 2D and 3D experiments, using X nucleus other than 13C or 15N Including: 31P/1H Heteronuclear COSY/TOCSY
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